Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001903.D Acq On : 22 May 2018 19:37 Operator : JC/MD Sample : PB109525ZHE#01 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 14 Sample Multiplier: 1 Quant Time: May 23 02:17:54 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 234978 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 315042 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 259171 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 112288 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 150951 47.93 ug/l 0.00 Spiked Amount 50.000 Recovery = 95.86% 35) Dibromofluoromethane 5.51 113 125153 47.07 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.14% 50) Toluene-d8 8.72 98 439299 46.14 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.28% 62) 4-Bromofluorobenzene 11.14 95 120339 35.10 ug/l 0.00 Spiked Amount 50.000 Recovery = 70.20% Target Compounds Qvalue 16) Acetone 2.45 43 7689 6.22 ug/l 98 18) Methyl Acetate 2.78 43 24781 6.85 ug/l 99 20) Methylene Chloride 2.86 84 8077 3.05 ug/l 97 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed