Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001904.D Acq On : 22 May 2018 20:04 Operator : JC/MD Sample : PB109525ZHE#02 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 15 Sample Multiplier: 1 Quant Time: May 23 02:20:15 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 239188 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 323194 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 268904 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 134327 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 158711 49.50 ug/l 0.00 Spiked Amount 50.000 Recovery = 99.00% 35) Dibromofluoromethane 5.51 113 129362 47.43 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.86% 50) Toluene-d8 8.72 98 454789 46.56 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.12% 62) 4-Bromofluorobenzene 11.14 95 132059 37.55 ug/l 0.00 Spiked Amount 50.000 Recovery = 75.10% Target Compounds Qvalue 16) Acetone 2.45 43 9124 7.25 ug/l 97 18) Methyl Acetate 2.78 43 25064 6.81 ug/l 97 20) Methylene Chloride 2.86 84 10447 3.88 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed