Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001905.D Acq On : 22 May 2018 20:31 Operator : JC/MD Sample : PB109525ZHE#12 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 16 Sample Multiplier: 1 Quant Time: May 23 02:22:32 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 229956 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 311319 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 263909 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 131257 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 151205 49.06 ug/l 0.00 Spiked Amount 50.000 Recovery = 98.12% 35) Dibromofluoromethane 5.51 113 123701 47.08 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.16% 50) Toluene-d8 8.72 98 439209 46.68 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.36% 62) 4-Bromofluorobenzene 11.15 95 129902 38.34 ug/l 0.00 Spiked Amount 50.000 Recovery = 76.68% Target Compounds Qvalue 16) Acetone 2.45 43 8677 7.17 ug/l 95 18) Methyl Acetate 2.78 43 26913 7.60 ug/l 99 20) Methylene Chloride 2.86 84 9766 3.77 ug/l 93 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed