Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001906.D Acq On : 22 May 2018 20:58 Operator : JC/MD Sample : PB109525ZHE#13 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 17 Sample Multiplier: 1 Quant Time: May 23 02:24:34 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 242052 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 328912 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 279580 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 139556 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 159892 49.28 ug/l 0.00 Spiked Amount 50.000 Recovery = 98.56% 35) Dibromofluoromethane 5.51 113 130583 47.04 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.08% 50) Toluene-d8 8.72 98 462814 46.56 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.12% 62) 4-Bromofluorobenzene 11.14 95 138327 38.65 ug/l 0.00 Spiked Amount 50.000 Recovery = 77.30% Target Compounds Qvalue 16) Acetone 2.45 43 8397 6.59 ug/l 100 18) Methyl Acetate 2.78 43 24769 6.65 ug/l 98 20) Methylene Chloride 2.86 84 10680 3.92 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed