Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001907.D Acq On : 22 May 2018 21:25 Operator : JC/MD Sample : PB109525ZHE#14 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 18 Sample Multiplier: 1 Quant Time: May 23 02:26:31 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 240060 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 328534 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 283387 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 147242 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 158897 49.38 ug/l 0.00 Spiked Amount 50.000 Recovery = 98.76% 35) Dibromofluoromethane 5.51 113 131838 47.55 ug/l 0.00 Spiked Amount 50.000 Recovery = 95.10% 50) Toluene-d8 8.72 98 466330 46.96 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.92% 62) 4-Bromofluorobenzene 11.14 95 138974 38.87 ug/l 0.00 Spiked Amount 50.000 Recovery = 77.74% Target Compounds Qvalue 16) Acetone 2.45 43 8784 6.95 ug/l 95 18) Methyl Acetate 2.78 43 24224 6.56 ug/l 100 20) Methylene Chloride 2.86 84 10791 3.99 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed