Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001908.D Acq On : 22 May 2018 21:52 Operator : JC/MD Sample : PB109525ZHE#15 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 19 Sample Multiplier: 1 Quant Time: May 23 02:28:46 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 238456 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 319996 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 271230 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 133290 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 155109 48.53 ug/l 0.00 Spiked Amount 50.000 Recovery = 97.06% 35) Dibromofluoromethane 5.51 113 128955 47.75 ug/l 0.00 Spiked Amount 50.000 Recovery = 95.50% 50) Toluene-d8 8.72 98 455420 47.09 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.18% 62) 4-Bromofluorobenzene 11.14 95 132686 38.10 ug/l 0.00 Spiked Amount 50.000 Recovery = 76.20% Target Compounds Qvalue 16) Acetone 2.45 43 9168 7.30 ug/l 90 18) Methyl Acetate 2.78 43 24457 6.66 ug/l 98 20) Methylene Chloride 2.86 84 10203 3.80 ug/l 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed