Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001909.D Acq On : 22 May 2018 22:18 Operator : JC/MD Sample : PB109525ZHE#16 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 20 Sample Multiplier: 1 Quant Time: May 23 02:31:00 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 236012 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 320630 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 262749 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 128515 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 154639 48.88 ug/l 0.00 Spiked Amount 50.000 Recovery = 97.76% 35) Dibromofluoromethane 5.51 113 127404 47.09 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.18% 50) Toluene-d8 8.72 98 451932 46.64 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.28% 62) 4-Bromofluorobenzene 11.14 95 126747 36.33 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.66% Target Compounds Qvalue 16) Acetone 2.45 43 9064 7.29 ug/l 100 18) Methyl Acetate 2.78 43 24884 6.85 ug/l 100 20) Methylene Chloride 2.86 84 6832 2.57 ug/l 93 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed