Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001910.D Acq On : 22 May 2018 22:45 Operator : JC/MD Sample : PB109525ZHE#17 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 21 Sample Multiplier: 1 Quant Time: May 23 03:08:11 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 240783 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 329350 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 286957 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 157113 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 158194 49.02 ug/l 0.00 Spiked Amount 50.000 Recovery = 98.04% 35) Dibromofluoromethane 5.51 113 130602 46.99 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.98% 50) Toluene-d8 8.72 98 465728 46.79 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.58% 62) 4-Bromofluorobenzene 11.14 95 143791 40.12 ug/l 0.00 Spiked Amount 50.000 Recovery = 80.24% Target Compounds Qvalue 16) Acetone 2.45 43 9344 7.37 ug/l 97 18) Methyl Acetate 2.78 43 23800 6.42 ug/l 100 20) Methylene Chloride 2.86 84 11848 4.37 ug/l 97 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed