Quantitation Report (QT/LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001915.D Acq On : 23 May 2018 01:25 Operator : JC/MD Sample : VX0522WBL02 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 27 Sample Multiplier: 1 Quant Time: May 23 03:27:24 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 302766 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 435152 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 374100 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 216987 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 234278 57.73 ug/l 0.00 Spiked Amount 50.000 Recovery = 115.46% 35) Dibromofluoromethane 5.51 113 192528 52.43 ug/l 0.00 Spiked Amount 50.000 Recovery = 104.86% 50) Toluene-d8 8.72 98 692745 52.67 ug/l 0.00 Spiked Amount 50.000 Recovery = 105.34% 62) 4-Bromofluorobenzene 11.14 95 219670 46.39 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.78% Target Compounds Qvalue -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed