Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001918.D Acq On : 23 May 2018 02:45 Operator : JC/MD Sample : PB109456TB Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 30 Sample Multiplier: 1 Quant Time: May 23 09:00:29 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 246474 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 329565 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 268109 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 141259 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 151597 45.89 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.78% 35) Dibromofluoromethane 5.51 113 125849 45.25 ug/l 0.00 Spiked Amount 50.000 Recovery = 90.50% 50) Toluene-d8 8.72 98 459342 46.11 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.22% 62) 4-Bromofluorobenzene 11.15 95 133894 37.33 ug/l 0.00 Spiked Amount 50.000 Recovery = 74.66% Target Compounds Qvalue 16) Acetone 2.45 43 9397 7.24 ug/l 98 18) Methyl Acetate 2.78 43 22770 6.00 ug/l 100 20) Methylene Chloride 2.86 84 6140 2.21 ug/l 94 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed