Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001919.D Acq On : 23 May 2018 03:12 Operator : JC/MD Sample : PB109525ZHE#19 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 31 Sample Multiplier: 1 Quant Time: May 23 03:52:34 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 257840 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 348058 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 296135 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 174526 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 162990 47.16 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.32% 35) Dibromofluoromethane 5.51 113 135202 46.03 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.06% 50) Toluene-d8 8.72 98 490642 46.64 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.28% 62) 4-Bromofluorobenzene 11.14 95 153057 40.41 ug/l 0.00 Spiked Amount 50.000 Recovery = 80.82% Target Compounds Qvalue 16) Acetone 2.45 43 7873 5.80 ug/l 100 18) Methyl Acetate 2.78 43 23284 5.87 ug/l 99 20) Methylene Chloride 2.86 84 7387 2.54 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed