Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001920.D Acq On : 23 May 2018 03:39 Operator : JC/MD Sample : PB109525ZHE#20 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 32 Sample Multiplier: 1 Quant Time: May 23 05:00:52 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 255313 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 351715 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 295869 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 172685 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 161892 47.31 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.62% 35) Dibromofluoromethane 5.51 113 134280 45.24 ug/l 0.00 Spiked Amount 50.000 Recovery = 90.48% 50) Toluene-d8 8.72 98 493151 46.39 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.78% 62) 4-Bromofluorobenzene 11.14 95 153775 40.18 ug/l 0.00 Spiked Amount 50.000 Recovery = 80.36% Target Compounds Qvalue 16) Acetone 2.45 43 8728 6.49 ug/l 98 18) Methyl Acetate 2.78 43 24430 6.22 ug/l 100 20) Methylene Chloride 2.86 84 8715 3.03 ug/l 95 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed