Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001921.D Acq On : 23 May 2018 04:06 Operator : JC/MD Sample : PB109456ZHE#01 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 33 Sample Multiplier: 1 Quant Time: May 23 05:02:58 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 256136 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 346640 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 296098 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 173115 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 161533 47.05 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.10% 35) Dibromofluoromethane 5.51 113 134148 45.86 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.72% 50) Toluene-d8 8.72 98 487324 46.51 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.02% 62) 4-Bromofluorobenzene 11.14 95 153031 40.57 ug/l 0.00 Spiked Amount 50.000 Recovery = 81.14% Target Compounds Qvalue 16) Acetone 2.45 43 9205 6.83 ug/l 99 18) Methyl Acetate 2.78 43 23061 5.85 ug/l 99 20) Methylene Chloride 2.86 84 5955 2.06 ug/l 90 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed