Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001922.D Acq On : 23 May 2018 04:32 Operator : JC/MD Sample : PB109456ZHE#02 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 34 Sample Multiplier: 1 Quant Time: May 23 05:05:04 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 248817 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 339854 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 283072 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 152576 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 157540 47.24 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.48% 35) Dibromofluoromethane 5.51 113 131827 45.96 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.92% 50) Toluene-d8 8.72 98 480532 46.78 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.56% 62) 4-Bromofluorobenzene 11.15 95 142112 38.42 ug/l 0.00 Spiked Amount 50.000 Recovery = 76.84% Target Compounds Qvalue 16) Acetone 2.45 43 9705 7.41 ug/l 99 18) Methyl Acetate 2.78 43 22130 5.78 ug/l 98 20) Methylene Chloride 2.86 84 5835 2.08 ug/l 94 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed