Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001924.D Acq On : 23 May 2018 05:26 Operator : JC/MD Sample : PB109456ZHE#04 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 36 Sample Multiplier: 1 Quant Time: May 23 06:52:45 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 246685 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 339256 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 288507 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 166378 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 158397 47.90 ug/l 0.00 Spiked Amount 50.000 Recovery = 95.80% 35) Dibromofluoromethane 5.51 113 131771 46.03 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.06% 50) Toluene-d8 8.72 98 481149 46.92 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.84% 62) 4-Bromofluorobenzene 11.14 95 147617 39.98 ug/l 0.00 Spiked Amount 50.000 Recovery = 79.96% Target Compounds Qvalue 16) Acetone 2.45 43 9541 7.35 ug/l 92 18) Methyl Acetate 2.78 43 23554 6.20 ug/l 98 20) Methylene Chloride 2.87 84 6430 2.31 ug/l 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed