Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001925.D Acq On : 23 May 2018 05:53 Operator : JC/MD Sample : PB109456ZHE#05 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 37 Sample Multiplier: 1 Quant Time: May 23 06:55:22 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 255616 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 351459 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 295856 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 173232 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 162819 47.52 ug/l 0.00 Spiked Amount 50.000 Recovery = 95.04% 35) Dibromofluoromethane 5.51 113 137175 46.25 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.50% 50) Toluene-d8 8.72 98 496887 46.78 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.56% 62) 4-Bromofluorobenzene 11.14 95 153593 40.16 ug/l 0.00 Spiked Amount 50.000 Recovery = 80.32% Target Compounds Qvalue 16) Acetone 2.45 43 9671 7.19 ug/l 93 18) Methyl Acetate 2.79 43 24548 6.24 ug/l 99 20) Methylene Chloride 2.86 84 6704 2.33 ug/l 97 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed