Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001926.D Acq On : 23 May 2018 06:19 Operator : JC/MD Sample : PB109456ZHE#06 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 38 Sample Multiplier: 1 Quant Time: May 23 06:57:35 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 248741 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 336484 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 278712 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 153724 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.08 65 156828 47.04 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.08% 35) Dibromofluoromethane 5.51 113 130586 45.99 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.98% 50) Toluene-d8 8.72 98 478019 47.00 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.00% 62) 4-Bromofluorobenzene 11.14 95 139452 38.08 ug/l 0.00 Spiked Amount 50.000 Recovery = 76.16% Target Compounds Qvalue 16) Acetone 2.45 43 8895 6.79 ug/l 96 18) Methyl Acetate 2.78 43 23335 6.10 ug/l 99 20) Methylene Chloride 2.86 84 6389 2.28 ug/l 97 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed