Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001927.D Acq On : 23 May 2018 06:46 Operator : JC/MD Sample : PB109456ZHE#10 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 39 Sample Multiplier: 1 Quant Time: May 23 11:51:34 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 250880 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 344187 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 284523 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 159891 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 159202 47.34 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.68% 35) Dibromofluoromethane 5.51 113 132665 45.67 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.34% 50) Toluene-d8 8.72 98 481372 46.27 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.54% 62) 4-Bromofluorobenzene 11.14 95 144328 38.53 ug/l 0.00 Spiked Amount 50.000 Recovery = 77.06% Target Compounds Qvalue 16) Acetone 2.45 43 9779 7.40 ug/l 97 18) Methyl Acetate 2.78 43 22464 5.82 ug/l 98 20) Methylene Chloride 2.86 84 7439 2.63 ug/l 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed