Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001928.D Acq On : 23 May 2018 07:13 Operator : JC/MD Sample : PB109456ZHE#11 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 40 Sample Multiplier: 1 Quant Time: May 23 11:53:34 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 256677 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 351713 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 300219 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 187531 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 161632 46.98 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.96% 35) Dibromofluoromethane 5.51 113 134485 45.31 ug/l 0.00 Spiked Amount 50.000 Recovery = 90.62% 50) Toluene-d8 8.72 98 498391 46.88 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.76% 62) 4-Bromofluorobenzene 11.14 95 158691 41.46 ug/l 0.00 Spiked Amount 50.000 Recovery = 82.92% Target Compounds Qvalue 16) Acetone 2.45 43 9995 7.40 ug/l 94 18) Methyl Acetate 2.78 43 22674 5.74 ug/l 99 20) Methylene Chloride 2.86 84 6956 2.40 ug/l 94 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed