Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001929.D Acq On : 23 May 2018 07:39 Operator : JC/MD Sample : PB109456ZHE#12 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 41 Sample Multiplier: 1 Quant Time: May 23 11:56:51 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 257112 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 347012 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 293958 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 177561 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 161047 46.73 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.46% 35) Dibromofluoromethane 5.51 113 133948 45.74 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.48% 50) Toluene-d8 8.72 98 496847 47.37 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.74% 62) 4-Bromofluorobenzene 11.14 95 152923 40.49 ug/l 0.00 Spiked Amount 50.000 Recovery = 80.98% Target Compounds Qvalue 16) Acetone 2.45 43 9607 7.10 ug/l 98 18) Methyl Acetate 2.79 43 21977 5.55 ug/l 100 20) Methylene Chloride 2.86 84 7469 2.58 ug/l 94 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed