Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001930.D Acq On : 23 May 2018 08:06 Operator : JC/MD Sample : PB109456ZHE#13 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 42 Sample Multiplier: 1 Quant Time: May 23 11:58:54 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 250471 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 338078 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 278020 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 152002 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 157179 46.82 ug/l 0.00 Spiked Amount 50.000 Recovery = 93.64% 35) Dibromofluoromethane 5.51 113 131462 46.08 ug/l 0.00 Spiked Amount 50.000 Recovery = 92.16% 50) Toluene-d8 8.72 98 480300 47.00 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.00% 62) 4-Bromofluorobenzene 11.14 95 139471 37.91 ug/l 0.00 Spiked Amount 50.000 Recovery = 75.82% Target Compounds Qvalue 16) Acetone 2.45 43 9182 6.96 ug/l 99 18) Methyl Acetate 2.78 43 23380 6.06 ug/l 100 20) Methylene Chloride 2.86 84 7127 2.53 ug/l 95 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed