Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052218\ Data File : VX001931.D Acq On : 23 May 2018 08:33 Operator : JC/MD Sample : PB109456ZHE#14 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 43 Sample Multiplier: 1 Quant Time: May 23 12:01:28 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X051518W.M Quant Title : SW846 8260 QLast Update : Tue May 15 01:36:22 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 254821 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 350153 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 298818 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 186352 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 162519 47.58 ug/l 0.00 Spiked Amount 50.000 Recovery = 95.16% 35) Dibromofluoromethane 5.51 113 135262 45.77 ug/l 0.00 Spiked Amount 50.000 Recovery = 91.54% 50) Toluene-d8 8.72 98 501010 47.34 ug/l 0.00 Spiked Amount 50.000 Recovery = 94.68% 62) 4-Bromofluorobenzene 11.14 95 158683 41.64 ug/l 0.00 Spiked Amount 50.000 Recovery = 83.28% Target Compounds Qvalue 16) Acetone 2.45 43 9695 7.23 ug/l 98 18) Methyl Acetate 2.79 43 22184 5.66 ug/l 98 20) Methylene Chloride 2.86 84 7455 2.60 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed