Quantitation Report (LSC Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002062.D Acq On : 27 May 2018 12:16 Operator : JC/MD Sample : VX0527WBL01 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 3 Sample Multiplier: 1 Quant Time: May 29 07:30:36 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 338571 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 468639 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 426767 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 237083 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 216212 35.73 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.46% 35) Dibromofluoromethane 5.51 113 172430 36.79 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.58% 50) Toluene-d8 8.72 98 671376 39.57 ug/l 0.00 Spiked Amount 50.000 Recovery = 79.14% 62) 4-Bromofluorobenzene 11.14 95 241050 36.31 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.62% Target Compounds Qvalue 3) Chloromethane 1.32 50 9639 1.85 ug/l # 87 20) Methylene Chloride 2.86 84 64932 14.89 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed