Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002066.D Acq On : 27 May 2018 14:13 Operator : JC/MD Sample : J2672-08 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 7 Sample Multiplier: 1 Quant Time: May 29 07:38:19 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 316771 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 433923 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 389222 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 218092 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 204601 36.13 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.26% 35) Dibromofluoromethane 5.51 113 159073 36.66 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.32% 50) Toluene-d8 8.72 98 618973 39.40 ug/l 0.00 Spiked Amount 50.000 Recovery = 78.80% 62) 4-Bromofluorobenzene 11.14 95 221592 36.05 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.10% Target Compounds Qvalue 16) Acetone 2.45 43 13301 6.09 ug/l 96 18) Methyl Acetate 2.78 43 23554 3.42 ug/l 94 20) Methylene Chloride 2.86 84 26796 5.60 ug/l 96 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed