Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002067.D Acq On : 27 May 2018 14:39 Operator : JC/MD Sample : J2678-04 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 8 Sample Multiplier: 1 Quant Time: May 29 07:42:17 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 320835 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 446373 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 402324 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 222283 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 210270 36.66 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.32% 35) Dibromofluoromethane 5.51 113 163630 36.66 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.32% 50) Toluene-d8 8.72 98 636585 39.39 ug/l 0.00 Spiked Amount 50.000 Recovery = 78.78% 62) 4-Bromofluorobenzene 11.14 95 227857 36.04 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.08% Target Compounds Qvalue 16) Acetone 2.45 43 11617 5.25 ug/l 92 18) Methyl Acetate 2.78 43 25709 3.77 ug/l 97 20) Methylene Chloride 2.86 84 21188 3.99 ug/l 99 95) Naphthalene 13.84 128 178596 8.90 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed