Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002068.D Acq On : 27 May 2018 15:06 Operator : JC/MD Sample : J3077-01 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 9 Sample Multiplier: 1 Quant Time: May 29 03:43:49 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 318438 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 447537 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 402930 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 223354 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 208056 36.55 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.10% 35) Dibromofluoromethane 5.51 113 153994 34.41 ug/l 0.00 Spiked Amount 50.000 Recovery = 68.82% 50) Toluene-d8 8.72 98 634277 39.15 ug/l 0.00 Spiked Amount 50.000 Recovery = 78.30% 62) 4-Bromofluorobenzene 11.14 95 227977 35.96 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.92% Target Compounds Qvalue 16) Acetone 2.45 43 20668 9.41 ug/l 99 20) Methylene Chloride 2.86 84 1207782 326.77 ug/l 98 95) Naphthalene 13.84 128 497816 24.68 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed