Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002069.D Acq On : 27 May 2018 15:32 Operator : JC/MD Sample : J3104-04 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 10 Sample Multiplier: 1 Quant Time: May 29 03:48:53 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 321851 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 450101 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 411850 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 223842 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 211066 36.69 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.38% 35) Dibromofluoromethane 5.51 113 164485 36.54 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.08% 50) Toluene-d8 8.72 98 641639 39.38 ug/l 0.00 Spiked Amount 50.000 Recovery = 78.76% 62) 4-Bromofluorobenzene 11.14 95 231580 36.32 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.64% Target Compounds Qvalue 16) Acetone 2.45 43 14108 6.35 ug/l 99 18) Methyl Acetate 2.78 43 23524 3.34 ug/l 98 20) Methylene Chloride 2.86 84 14003 2.04 ug/l 97 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed