Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002070.D Acq On : 27 May 2018 15:59 Operator : JC/MD Sample : J3104-02 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 11 Sample Multiplier: 1 Quant Time: May 29 03:52:29 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 314194 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 439011 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 396074 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 215861 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 205624 36.61 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.22% 35) Dibromofluoromethane 5.51 113 159543 36.34 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.68% 50) Toluene-d8 8.72 98 625017 39.32 ug/l 0.00 Spiked Amount 50.000 Recovery = 78.64% 62) 4-Bromofluorobenzene 11.14 95 222531 35.79 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.58% Target Compounds Qvalue 16) Acetone 2.45 43 16011 7.39 ug/l 96 18) Methyl Acetate 2.78 43 22190 3.19 ug/l 96 20) Methylene Chloride 2.86 84 41107 9.61 ug/l 97 95) Naphthalene 13.84 128 25198 1.29 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed