Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002071.D Acq On : 27 May 2018 16:25 Operator : JC/MD Sample : J3099-06 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 12 Sample Multiplier: 1 Quant Time: May 29 03:55:44 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 320445 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 454749 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 412675 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 236568 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 213269 37.23 ug/l 0.00 Spiked Amount 50.000 Recovery = 74.46% 35) Dibromofluoromethane 5.51 113 166046 36.51 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.02% 50) Toluene-d8 8.72 98 642613 39.03 ug/l 0.00 Spiked Amount 50.000 Recovery = 78.06% 62) 4-Bromofluorobenzene 11.14 95 235554 36.57 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.14% Target Compounds Qvalue 16) Acetone 2.45 43 18326 8.29 ug/l 97 18) Methyl Acetate 2.78 43 26890 4.00 ug/l 99 20) Methylene Chloride 2.86 84 6580497 1776.84 ug/l 95 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed