Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002072.D Acq On : 27 May 2018 16:52 Operator : JC/MD Sample : J3099-03 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 13 Sample Multiplier: 1 Quant Time: May 29 03:59:06 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 320306 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 453676 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 408944 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 230675 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 210769 36.81 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.62% 35) Dibromofluoromethane 5.51 113 163412 36.02 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.04% 50) Toluene-d8 8.72 98 642644 39.13 ug/l 0.00 Spiked Amount 50.000 Recovery = 78.26% 62) 4-Bromofluorobenzene 11.14 95 232265 36.14 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.28% Target Compounds Qvalue 16) Acetone 2.45 43 18709 8.47 ug/l 100 18) Methyl Acetate 2.78 43 24140 3.48 ug/l 96 20) Methylene Chloride 2.86 84 1110653 298.59 ug/l 98 95) Naphthalene 13.84 128 302291 14.51 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed