Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002073.D Acq On : 27 May 2018 17:18 Operator : JC/MD Sample : J2679-28 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 14 Sample Multiplier: 1 Quant Time: May 29 04:02:37 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 319980 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 447550 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 408775 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 236654 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 210997 36.89 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.78% 35) Dibromofluoromethane 5.51 113 162223 36.25 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.50% 50) Toluene-d8 8.72 98 638678 39.42 ug/l 0.00 Spiked Amount 50.000 Recovery = 78.84% 62) 4-Bromofluorobenzene 11.14 95 235946 37.22 ug/l 0.00 Spiked Amount 50.000 Recovery = 74.44% Target Compounds Qvalue 16) Acetone 2.45 43 18458 8.36 ug/l 98 18) Methyl Acetate 2.78 43 25433 3.73 ug/l 100 20) Methylene Chloride 2.86 84 5404541 1461.12 ug/l 95 84) 1,2,4-Trimethylbenzene 11.81 105 34381 1.94 ug/l 100 95) Naphthalene 13.84 128 60244 2.82 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed