Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002074.D Acq On : 27 May 2018 17:45 Operator : JC/MD Sample : J2679-30 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 15 Sample Multiplier: 1 Quant Time: May 29 04:09:27 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 313013 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 439875 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 397416 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 222546 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 204947 36.63 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.26% 35) Dibromofluoromethane 5.51 113 158257 35.98 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.96% 50) Toluene-d8 8.72 98 628842 39.49 ug/l 0.00 Spiked Amount 50.000 Recovery = 78.98% 62) 4-Bromofluorobenzene 11.14 95 224389 36.01 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.02% Target Compounds Qvalue 16) Acetone 2.45 43 19057 8.83 ug/l 97 18) Methyl Acetate 2.78 43 24491 3.65 ug/l 98 20) Methylene Chloride 2.86 84 99797 25.89 ug/l 98 84) 1,2,4-Trimethylbenzene 11.81 105 40618 2.44 ug/l 98 95) Naphthalene 13.84 128 116804 5.81 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed