Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002075.D Acq On : 27 May 2018 18:11 Operator : JC/MD Sample : J2679-26 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 16 Sample Multiplier: 1 Quant Time: May 29 04:13:16 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 320345 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 442996 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 401658 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 225931 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 207254 36.19 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.38% 35) Dibromofluoromethane 5.51 113 160462 36.22 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.44% 50) Toluene-d8 8.72 98 632491 39.44 ug/l 0.00 Spiked Amount 50.000 Recovery = 78.88% 62) 4-Bromofluorobenzene 11.14 95 225819 35.99 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.98% Target Compounds Qvalue 16) Acetone 2.45 43 16145 7.31 ug/l 96 18) Methyl Acetate 2.78 43 23109 3.28 ug/l 100 20) Methylene Chloride 2.86 84 62307 15.12 ug/l 100 95) Naphthalene 13.84 128 33266 1.63 ug/l 98 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed