Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002076.D Acq On : 27 May 2018 18:38 Operator : JC/MD Sample : J3130-02 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 17 Sample Multiplier: 1 Quant Time: May 29 08:31:08 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 316277 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 435206 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 399760 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.08 152 221673 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 204868 36.24 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.48% 35) Dibromofluoromethane 5.51 113 158572 36.44 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.88% 50) Toluene-d8 8.72 98 628933 39.92 ug/l 0.00 Spiked Amount 50.000 Recovery = 79.84% 62) 4-Bromofluorobenzene 11.14 95 224700 36.45 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.90% Target Compounds Qvalue 16) Acetone 2.45 43 15405 7.06 ug/l 97 18) Methyl Acetate 2.78 43 24529 3.61 ug/l 99 20) Methylene Chloride 2.86 84 69181 17.22 ug/l 99 44) Trichloroethene 7.22 130 11189 2.17 ug/l 96 68) m/p-Xylenes 10.36 106 9050 1.08 ug/l 99 95) Naphthalene 13.84 128 514176 25.68 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed