Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002077.D Acq On : 27 May 2018 19:04 Operator : JC/MD Sample : J3130-04 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 18 Sample Multiplier: 1 Quant Time: May 29 08:33:24 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 323204 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 450212 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 403878 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 219738 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 213237 36.91 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.82% 35) Dibromofluoromethane 5.51 113 164080 36.44 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.88% 50) Toluene-d8 8.72 98 640329 39.29 ug/l 0.00 Spiked Amount 50.000 Recovery = 78.58% 62) 4-Bromofluorobenzene 11.14 95 224461 35.20 ug/l 0.00 Spiked Amount 50.000 Recovery = 70.40% Target Compounds Qvalue 16) Acetone 2.45 43 15789 7.08 ug/l 99 18) Methyl Acetate 2.78 43 27834 4.14 ug/l 100 20) Methylene Chloride 2.86 84 67318 16.31 ug/l 97 84) 1,2,4-Trimethylbenzene 11.81 105 27123 1.65 ug/l 99 95) Naphthalene 13.84 128 528369 26.62 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed