Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002078.D Acq On : 27 May 2018 19:31 Operator : JC/MD Sample : J3130-06 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 19 Sample Multiplier: 1 Quant Time: May 29 08:37:18 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 318574 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 444370 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 402916 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 227171 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 208296 36.58 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.16% 35) Dibromofluoromethane 5.51 113 162589 36.59 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.18% 50) Toluene-d8 8.72 98 634935 39.47 ug/l 0.00 Spiked Amount 50.000 Recovery = 78.94% 62) 4-Bromofluorobenzene 11.14 95 228485 36.30 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.60% Target Compounds Qvalue 8) Diethyl Ether 2.19 74 8910 3.46 ug/l 100 16) Acetone 2.45 43 19044 8.67 ug/l 98 18) Methyl Acetate 2.78 43 25198 3.71 ug/l 97 20) Methylene Chloride 2.86 84 64445 15.80 ug/l 97 84) 1,2,4-Trimethylbenzene 11.81 105 23927 1.41 ug/l 98 95) Naphthalene 13.84 128 531383 25.90 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed