Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002079.D Acq On : 27 May 2018 19:58 Operator : JC/MD Sample : J3130-08 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 20 Sample Multiplier: 1 Quant Time: May 29 04:29:56 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 321078 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 455932 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 408648 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 227246 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 214003 37.29 ug/l 0.00 Spiked Amount 50.000 Recovery = 74.58% 35) Dibromofluoromethane 5.51 113 164769 36.14 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.28% 50) Toluene-d8 8.72 98 641113 38.84 ug/l 0.00 Spiked Amount 50.000 Recovery = 77.68% 62) 4-Bromofluorobenzene 11.14 95 231497 35.85 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.70% Target Compounds Qvalue 16) Acetone 2.45 43 15826 7.15 ug/l 97 18) Methyl Acetate 2.78 43 28787 4.36 ug/l 97 20) Methylene Chloride 2.86 84 128783 33.01 ug/l 98 25) 2-Butanone 4.71 43 5108 1.26 ug/l 100 84) 1,2,4-Trimethylbenzene 11.81 105 20526 1.21 ug/l 100 95) Naphthalene 13.84 128 227190 11.07 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed