Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002080.D Acq On : 27 May 2018 20:24 Operator : JC/MD Sample : J3128-03 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 21 Sample Multiplier: 1 Quant Time: May 29 08:46:28 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 305135 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 428445 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 382885 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 207739 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 198211 36.34 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.68% 35) Dibromofluoromethane 5.51 113 153455 35.82 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.64% 50) Toluene-d8 8.72 98 601131 38.75 ug/l 0.00 Spiked Amount 50.000 Recovery = 77.50% 62) 4-Bromofluorobenzene 11.14 95 212016 34.93 ug/l 0.00 Spiked Amount 50.000 Recovery = 69.86% Target Compounds Qvalue 16) Acetone 2.45 43 13114 6.23 ug/l 91 18) Methyl Acetate 2.78 43 26220 4.13 ug/l 99 20) Methylene Chloride 2.86 84 26979 5.93 ug/l 98 95) Naphthalene 13.84 128 105440 5.62 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed