Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002081.D Acq On : 27 May 2018 20:51 Operator : JC/MD Sample : J3128-06 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 22 Sample Multiplier: 1 Quant Time: May 29 08:49:12 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 302227 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 414716 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 375005 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 205581 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 196216 36.32 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.64% 35) Dibromofluoromethane 5.51 113 150240 36.23 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.46% 50) Toluene-d8 8.72 98 593215 39.51 ug/l 0.00 Spiked Amount 50.000 Recovery = 79.02% 62) 4-Bromofluorobenzene 11.14 95 208837 35.55 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.10% Target Compounds Qvalue 16) Acetone 2.45 43 15161 7.27 ug/l 97 18) Methyl Acetate 2.78 43 25635 4.06 ug/l 95 20) Methylene Chloride 2.86 84 783154 222.70 ug/l 98 95) Naphthalene 13.84 128 371529 20.01 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed