Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002082.D Acq On : 27 May 2018 21:17 Operator : JC/MD Sample : J3114-03 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 23 Sample Multiplier: 1 Quant Time: May 29 08:52:40 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 329299 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 463192 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 431518 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 248140 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 216787 36.83 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.66% 35) Dibromofluoromethane 5.51 113 168973 36.48 ug/l 0.00 Spiked Amount 50.000 Recovery = 72.96% 50) Toluene-d8 8.72 98 666613 39.75 ug/l 0.00 Spiked Amount 50.000 Recovery = 79.50% 62) 4-Bromofluorobenzene 11.14 95 247081 37.66 ug/l 0.00 Spiked Amount 50.000 Recovery = 75.32% Target Compounds Qvalue 16) Acetone 2.45 43 18557 8.17 ug/l 95 20) Methylene Chloride 2.82 84 48794150m 12831.65 ug/l 28) Bromochloromethane 5.04 49 23071 5.22 ug/l 98 95) Naphthalene 13.84 128 98485 4.39 ug/l 99 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed