Quantitation Report (QT Reviewed) Data Path : W:\HPCHEM1\MSVOA_X\DATA\VX052718\ Data File : VX002083.D Acq On : 27 May 2018 21:44 Operator : JC/MD Sample : J3114-07 Misc : 5.0mL/MSVOA_X/WATER ALS Vial : 24 Sample Multiplier: 1 Quant Time: May 29 08:56:17 2018 Quant Method : W:\HPCHEM1\MSVOA_X\METHOD\82X052418W.M Quant Title : SW846 8260 QLast Update : Thu May 24 13:09:03 2018 Response via : Initial Calibration Internal Standards R.T. QIon Response Conc Units Dev(Min) -------------------------------------------------------------------------- 1) Pentafluorobenzene 5.67 168 313926 50.00 ug/l 0.00 34) 1,4-Difluorobenzene 6.87 114 440311 50.00 ug/l 0.00 63) Chlorobenzene-d5 10.12 117 391323 50.00 ug/l 0.00 72) 1,4-Dichlorobenzene-d4 12.09 152 216881 50.00 ug/l 0.00 System Monitoring Compounds 33) 1,2-Dichloroethane-d4 6.07 65 207787 37.03 ug/l 0.00 Spiked Amount 50.000 Recovery = 74.06% 35) Dibromofluoromethane 5.51 113 161980 36.79 ug/l 0.00 Spiked Amount 50.000 Recovery = 73.58% 50) Toluene-d8 8.72 98 619271 38.85 ug/l 0.00 Spiked Amount 50.000 Recovery = 77.70% 62) 4-Bromofluorobenzene 11.14 95 221903 35.58 ug/l 0.00 Spiked Amount 50.000 Recovery = 71.16% Target Compounds Qvalue 16) Acetone 2.45 43 23219 10.72 ug/l 98 18) Methyl Acetate 2.78 43 28459 4.42 ug/l 98 20) Methylene Chloride 2.86 84 252740 68.00 ug/l 98 95) Naphthalene 13.84 128 266993 13.63 ug/l 100 -------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration (+) = signals summed